Classification of Experiments This book now contains a multitude of different experiments with many different purposes. The following classification should help the reader to select one for the desired application: Calibration Experiments are all those where you want to determine instrumental values for further use in your applications. To these belong especially: Exps. 2.1 – 2.5, 4.1 – 4.3, 5.1 – 5.2, 7.1 – 7.3, 11.1, 11.6, 14.2 – 14.3, 15.1

Maintenance Experiments are all those, that you perform to correct for instrument aging or malfunction. To these belong especially: Exps. 3.5 – 3.13, 11.2-11.4 Standard Organic Experiments. There is a typical sequence of experiments that are routinely performed during organic structure elucidation. To these belong especially: Exps. 3.1, 3.2, 6.11, 12.1, 12.8, 12.5, 12.19 Spin Coupling Experiments are those where the aim is to determine the numerical value of a spin coupling constant. To these belong especially:

Exps. 3.4, 4.12, 4.14, 6.13, 7.10, 10.5 – 10.7, 10.19, 10.23, 11.14, 11.15, 12.13, 12.14, 15.20 Dipolar Coupling Experiments are those where the aim is to determine the distance between spins in space via Overhauser-type measurements. To these belong especially: Exps. 4.8 – 4.10, 4.16, 8.13, 10.20 – 10.22, 11.12, 12.19 – 12.21, 14.8, 15.17 - 15.19 Solvent Suppression Experiments are those where one tries to remove the solvent signals. To these belong especially: Exps. 6.18 – 6.19, 8.9, 10.8, 11.16 – 11.18